3-METHOXY THIOANISOL

Name	3-Methoxy thioanisole
Synonyms	m-Methylthioanisole 3-Methoxythioanisole 3-METHOXY THIOANISOL 3-Methoxy thioanisole 3-METHOXY THIOANISOLE Anisole, m-(methylthio)- Anisole, m- (methylthio)- 1-Methoxy-3-methylthiobenzene 1-Methoxy-3-(methylthio)benzene 1-(Methylthio)-3-methoxybenzene (3-methoxyphenyl)(methyl)sulfane 1-methoxy-3-methylsulfanylbenzene Benzene, 1-methoxy-3-(methylthio)- 1-methoxy-3-methylsulfanyl-benzene 1-Methoxy-3-(methylsulfanyl)benzene Benzene, 1-methoxy-3- (methylthio)- Methyl 3-(methylsulfanyl)phenyl ether
CAS	2388-74-1
InChI	InChI=1/C8H10O2S/c1-9-7-4-3-5-8(6-7)11-10-2/h3-6H,1-2H3

Molecular Formula	C8H10OS
Molar Mass	154.23
Density	1.12
Boling Point	127 °C / 18mmHg
Storage Condition	Room Temprature
Refractive Index	1.5820 to 1.5860
MDL	MFCD03789162
Physical and Chemical Properties	Colorless to light yellow liquid.

Hazard Symbols	Xi - Irritant
Hazard Class	IRRITANT, STENCH

Application	3-methoxyanisthioether is an organic intermediate, which can be obtained by alkylation of 3-(methylthio) phenol and methyl iodide or prepared by nucleophilic substitution of 3-chloroanisole with sodium methanolate.
Preparation	In order to stir and dissolve 3-(methylthio) phenol (1g,7.13mmol) into acetonitrile (10mL), potassium carbonate (1.972g,14.27mmol) was added at 0°C. The reactants were stirred for 20 minutes, and then methyl iodide (0.9mL,14.27mmol) was added dropwise to the reaction mixture. The reaction mixture was heated to 45°C for 8 hours. After the reaction is completed, acetonitrile is evaporated. The crude reaction mixture was placed in ethyl acetate (50mL) and washed with a saline solution. The organic layer was separated and dried, filtered and concentrated with anhydrous sodium sulfate to obtain 3-methoxyanisethiole (0.935g, yield 85%).
chemical properties	colorless to light yellow liquid.
NIST chemical information	information provided by: webbook.nist.gov (external link)

Last Update：2024-04-09 19:05:04

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3-METHOXY THIOANISOL

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